Data File D:\\AGLIENT 1260\\DATA\\20150826\\20150826 2015-08-26 09-07-31\\BIZ2015-826-DJL6.DSample Name: BIZ2015-826-DJL6=====================================================================Acq. Operator : Li Shan(LCMS-02) Seq. Line : 30Acq. Instrument : HY-LCMS-02 Location : P1-C-09Injection Date : 8/26/2015 11:34:55 AM Inj : 1 Inj Volume : 3.000 µlAcq. Method : D:\\AGLIENT 1260\\DATA\\20150826\\20150826 2015-08-26 09-07-31\\100-1000MS+3MIN- 1.5_(0.02%FA).MLast changed : 8/26/2015 9:07:31 AM by Li Shan(LCMS-02)Analysis Method : D:\\AGLIENT 1260\\DATA\\20150825\\20150825 2015-08-25 09-11-32\\100-1000MS+3MIN- 1.5_(0.02%FA).M (Sequence Method)Last changed : 8/26/2015 1:11:51 PM by Li Shan(LCMS-02) (modified after loading)Method Info : Postive,MS:100-1000,Column ID:A-RP-132,40℃ Catalog No : HY-13812 Batch#17659 A-RP-134 Additional Info : Peak(s) manually integrated DAD1 C, Sig=254,4 Ref=off (D:\\AGLIENT...60\\DATA\\20150826\\20150826 2015-08-26 09-07-31\\BIZ2015-826-DJL6.D) 1.923 1.666mAU12001000800600400 2.161 1.54920000.51 1.380 1.832 2.2811.522.53min ===================================================================== Area Percent Report ===================================================================== Sorted By : SignalMultiplier : 1.0000Dilution : 1.0000Do not use Multiplier & Dilution Factor with ISTDs Signal 1: DAD1 C, Sig=254,4 Ref=off Peak RetTime Type Width Area Height Area # [min] [min] [mAU*s] [mAU] %----|-------|----|-------|----------|----------|--------| 1 1.380 MM 0.0663 2.24252 5.63502e-1 0.0350 2 1.549 MM 0.0454 13.32038 4.89490 0.2078 3 1.666 MM 0.0463 34.04598 12.26233 0.5310 4 1.832 MF 0.0385 1.83185 7.93981e-1 0.0286 5 1.923 FM 0.0749 6347.26367 1412.62170 98.9989 6 2.161 FM 0.0474 10.49444 3.68877 0.1637 7 2.281 MM 0.0445 2.24838 8.41281e-1 0.0351 Totals : 6411.44721 1435.66647 ===================================================================== *** End of Report ***HY-LCMS-02 8/26/2015 1:11:53 PM Li Shan(LCMS-02)Page 1 of 1
Data File D:\\AGLIENT 1260\\DATA\\20150826\\20150826 2015-08-26 09-07-31\\BIZ2015-826-DJL6.DSample Name: BIZ2015-826-DJL6=====================================================================Acq. Operator : Li Shan(LCMS-02) Seq. Line : 30Acq. Instrument : HY-LCMS-02 Location : P1-C-09Injection Date : 8/26/2015 11:34:55 AM Inj : 1 Inj Volume : 3.000 µlAcq. Method : D:\\AGLIENT 1260\\DATA\\20150826\\20150826 2015-08-26 09-07-31\\100-1000MS+3MIN- 1.5_(0.02%FA).MLast changed : 8/26/2015 9:07:31 AM by Li Shan(LCMS-02)Analysis Method : D:\\AGLIENT 1260\\DATA\\20150825\\20150825 2015-08-25 09-11-32\\100-1000MS+3MIN- 1.5_(0.02%FA).M (Sequence Method)Last changed : 8/26/2015 1:13:01 PM by Li Shan(LCMS-02) (modified after loading)Method Info : Postive,MS:100-1000,Column ID:A-RP-132,40℃ Catalog No : HY-13812 Batch#17659 A-RP-134 Additional Info : Peak(s) manually integrated MSD1 TIC, MS File (D:\\AGLIENT 1260\\DATA\\20150826\\20150826 2015-08-26 09-07-31\\BIZ2015-826-DJL6.D) ES-API, Pos, Sca 1.93314000001200000100000080000060000040000020000000.511.522.53min HY-LCMS-02 8/26/2015 1:13:03 PM Li Shan(LCMS-02)Page 1 of 2
Data File D:\\AGLIENT 1260\\DATA\\20150826\\20150826 2015-08-26 09-07-31\\BIZ2015-826-DJL6.DSample Name: BIZ2015-826-DJL6MS Signal: MSD1 TIC, MS File, ES-API, Pos, Scan, Frag: 50 Spectra averaged over upper half of peaks. Noise Cutoff: 1000 counts. Reportable Ion Abundance: > 10%. Retention Mol. WeightTime (MS) MS Area or Ion 1.933 10421151 358.10 I 357.15 I*MSD1 SPC, time=1.889:1.999 of D:\\AGLIENT 1260\\DATA\\20150826\\20150826 2015-08-26 09-07-31\\BIZ2015-826-DJL6.D ES-API,100806040200100200300400500600700800m/z 357.1Max: 871360 *** End of Report ***HY-LCMS-02 8/26/2015 1:13:03 PM Li Shan(LCMS-02) 358.1Page 2 of 2